Shimadzu aa 7000 руководство по эксплуатации

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Summary of Contents for Shimadzu AA-7000 Series

System Configuration can Evolve

with Your Needs

The AA-7000 Series can be upgraded by adding units to allow the system to handle the analysis targets.

The AA-7000 Series can be upgraded by adding units to allow the system to handle the analysis targets.

AA-7000G

Major Fields of Application

AA-7000 Series supports a wide range of

analysis applications.

Environment

Seawater, river water, effluent,

sludge, air-borne dust

Metals, Semiconductors, Ceramics

Metals, minerals, glass,

ceramics, IC chips

Petroleum, Chemicals, Polymers

Petroleum, oil, catalysts,

chemical products, biodiesel

Medical, Biology, Pharmaceuticals

Blood, animals, plants,

drugs, food products

4

AA — 7000F

AA-7000F/AAC

GFA-7000A

ASC

*1

AA-7000F Manual Burner System

ASC

*1

AA-7000F/AAC Auto Burner System

ASC

*2

AA-7000G

GFA-7000A Auto Sampler System

Analysis Sensitivities

Concentration limit of detection

H

Li

Be

Na

Mg

K

Ca Sc Ti

V

Cr Mn Fe Co Ni Cu Zn

Rb Sr

Y Zr Nb Mo Tc Ru Rh Pd

Cs Ba La

Hf Ta W Re Os Ir

Fr Ra Ac

Ce Pr Nd Pm Sm Eu Gd Tb

Th Pa U Np Pu Am Cm Bk

* May differ according to coexisting substances in the sample.

AAC

AAC

*3

Flame

Furnace

(ppm)

B

C

N

O

Al

Si

P

S

Ga

a

Ge As

Se

Ag

Cd

In

Sn Sb

Te

Pt

Au

Hg

Tl

Pb

Bi

Po

Dy

Ho

Er

Tm

Cf

Es

Fm

Md

GFA

*2

(ppb)

He

F

Ne

Cl

Ar

Br

Kr

I

Xe

At

Rn

Yb

Lu

No

Lr

• 24, Shimadzu AA-7000 Series Specifications Basics Main Unit Flame Furnace (GFA-7000A) Wavelength range 185.0 to 900.0 nm Aberration-corrected Czerny-Turner mounting, Number of grating grooves: 1800 lines / mm, Focal length: 300 mm 0.2, 0.7, 1.3, 2.0L nm (4-step automatic switching) . BGC-SR (high-speed self-reversal method) (185.0 to 900.0 nm) . BGC-D2 (D 2 lamp method) (185.0 to 430.0 nm) 6-lamp turret, 2…

• 25, Shimadzu AA-7000 Series * Notes . The PC, monitor and printer are not included in the standard configuration. Prepare them separately. . The ASC-7000, ASK-7000 and GFA-7000A are optional accessories. . The separately available micro sampling kit is required for the flame micro sampling method. . Microsoft Windows 7 Professional / Vista Business and XP Professional are registered trademarks of Micros…

• 5, 5 Flame and Measurement Procedures Flame Selection Air-C2H2 N2O-C2H2 HVG MVU H Be NeFONCB Na Mg ArClSPAl KCa Ti CrMnFeCoNiCuZn KrBrGa Rb Sr Y Zr Nb Mo Tc Ru Rh Pd Cd XeITeIn Cs Ba La Fr Ra Ac Hf Ta W Re Os Ir Pt Au RnAtPoBiPbTl Ce Pr Nd Pm Sm Eu Gd Tb LuYbTmErHoDy Th Pa U Np Pu Am Cm Bk LrNoMdFmEsCf He Ag u Ge Si V Li SeAs Sb Hg Sc Sn H HVG AUTO Graphite Furnace Atomizer GFA AA-7000F/AAC Dua…

• 17, Software Provides Comprehensive Information Displays and Flexible Settings Identical software operation for flame and furnace measurements Combining a high-performance autosampler simplifies advanced settings Even if the calibration curve is created after sample measurements, concentration calculations can be conducted on past data. This allows trial measure…

• 18, FDA 21 CFR Part 11 Compliance FDA 21 CFR Part 11 Compliance Supports System Management andAccuracy FDA 21 CFR Part 11 Compliance A combination of enhanced WizAArd software with Shimadzu’s network-compatible CLASS-Agent data management software supports FDA 21 CFR Part 11 Compliance. WizAArd used alone provides comprehensive system policy sett…

• 7, 7 Advantages of the Double-Beam System Support for Developing Analytical Conditions Optional Autosampler Reduces Analysis Workload Long-term stability The graph shows the results of measurements on 2 ppm copper (Cu) conducted over at least one hour. (The plot shows mean values for 11 repeated measurements.) Over the course of more than 600 measurements, th…

• 9, High-Performance Autosampler High-Sensitivity Application Data (Analysis of Selenium (Se)) Mix and inject up to four sample types (diluted solution, standard solution, sample, matrix modifier, etc.). (Of course, unmixed samples can also be injected.) Select a fluororesin tube or pipette tip as the injection nozzle. Automatic dilution and re-analysis if the calibration curve co…

• 10, Shimadzu AA-7000 Series AA-7000F/AAC creates an integral burner and furnace that remains permanently installed in the combustion chamber. It supports both flame analysis of high concentration samples and furnace analysis of trace samples, without changing the atomizer unit. The integral construction with the atomizer saves space. AA-7000F enables above function by AAC-7000 (option). * The AAC-70…

• 6, Detector Hollow cathode lamp Beam splitter Monochromator D2 lamp Chopper mirror Burner head (or graphite tube) Reference beam Sample beam 6 Enhanced Flame Analysis The AA-7000 Series incorporates newly developed 3D double-beam optics. The optical system has been designed to produce its maximum performance for each measurement method through optimal adjustment of the light beam and lig…

• 20, Standard Parts / PC / Software 20 * The PC, monitor, printer, hollow cathode lamps, high-temperature burner head, pressure regulator and compressor are not included in the standard configuration. Part Name Quantity P/N 071-60821-08 (120 V), 071-60825-51 (230 V)1 206-52046-911 1 206-97176 Common to All AA-7000 Series Models 1 206-97225 1 228-30164 1 037-70238-01 1…

• 12, Safety is an extremely important consideration for flame atomic absorption spectrophotometers using acetylene gas. The AA-7000 Series instruments are the first* ones in the world fitted with a vibration sensor as standard. They also incorporate a comprehensive range of safety mechanisms, including gas leak detectors. * Shimadzu in-house investigation. Current as of November 2008. Comp…

• 15, Shimadzu AA-7000 Series D 2 (deuterium lamp) method –– highly sensitive background correction 1. Detection sensitivity is superior to the SR method. Therefore, this method is suitable for the analysis of samples with a simple matrix requiring high sensitivity, such as the measurement of trace levels of impurities in ultrapure water or environmental analyses. 2. As the lighting frequency is higher than with the …

• 147LPQ OPERATING MANUAL EM-9516-B Rev.10Digital Panel Meters 47 SeriesPULSE INPUT TOTALIZER(6-digit, LED display type)Model: 47LPQOPERATING MANUALhttp://www.m-system.co.jp/5-2-55, Minamitsumori, Nishinari-ku, Osaka 557-0063 JAPANTe l: +81-6-6659-8201 Fax: +81-6-6659-8510E-mail: [email protected] …

  47 Series 137

•  Vor Gebrauch lesen! / Read manual before use! / Przeczytać przed użyciem!  Alle Sicherheitshinweise beachten! / Observe all safety information! / Przestrzegać wszystkich wskazówek bezpieczeństwa!  Für künftige Verwendung aufbewahren! / Keep manual for future use! / Przechowywać do przyszłego wykorzystania! 06.2015 0 854.000.0740 Betriebsan …

  DIT 10 67

• Model 72-8155: OPERATING MANUAL1Table of ContentsTitle PageOverviewInspectionSafety InformationRules For Safe OperationInternational Electrical SymbolsThe Meter StructureFunctional ButtonsDisplay SymbolsMeasurement Operation A. Measuring Resistance B. Diode and Continuity Test C. Capacitance Measurement D. Inductance Measurement E. …

  72-8155 26

• Heinrichs Messtechnik GmbH OPERATING MANUAL TMU-W / UMC4 November 2020 High-Pressure Coriolis Mass Flow Meter TMU-W Installation and operation manual Please read the instructions carefully and store them in a safe place …

  Heinrichs TMU-W Series 118

• High-Performance Autosampler High-Sensitivity Application Data (Analysis of Selenium (Se)) Mix and inject up to four sample types (diluted solution, standard solution, sample, matrix modifier, etc.). (Of course, unmixed samples can also be injected.) Select a fluororesin tube or pipette tip as the injection nozzle. Automatic dilution and re-analysis if the calibration curve concentration is exceeded. Independent control o

• D 2 (deuterium lamp) method –– highly sensitive background correction 1. Detection sensitivity is superior to the SR method. Therefore, this method is suitable for the analysis of samples with a simple matrix requiring high sensitivity, such as the measurement of trace levels of impurities in ultrapure water or environmental analyses. 2. As the lighting frequency is higher than with the SR method, it can eliminate noise due to emission components of the flame or graphite tube to permit accu

• 21 High-density graphite tube 206-50587-11 Pyro-coated graphite tube Platform tube 206-50588-11 Select one of the three types of graphite tubes according to the aim of the analysis. 206-50887-02 MAF-106S compressed gas regulator 040-72019-21 For Argon gas I Specifications GFA-7000A graphite furnace atomizer 206-77777-XX For Furnace Analysis For cooling GFA, 100 VAC, 1100VA, 50/60 Hz CA-1115A-1 cooling water circulation unit 044-01813-01 For connecting GFA and CA-1115A-1Cooler connection kit Parts for cooling water con

• The optimal background correction methods are installed as standard: high-speed self-reversal method (SR method) and deuterium lamp method (D 2 method). Dual-Background Correction Functions SR (high-speed self-reversal) method –– accurate background correction over a wide range Samples with a complex matrix (Containing a large quantity of a specific element as the main component) Purified water, tap water, environmental water, etc. Samples with a relatively simple matrix Samples suitable for the SR me

• FDA 21 CFR Part 11 Compliance FDA 21 CFR Part 11 Compliance Supports System Management andAccuracy FDA 21 CFR Part 11 Compliance A combination of enhanced WizAArd software with Shimadzu’s network-compatible CLASS-Agent data management software supports FDA 21 CFR Part 11 Compliance. WizAArd used alone provides comprehensive system poli

• For High-Sensitivity Hg Analysis MVU-1A mercury vaporizer unit 206-58780-XX This mercury vaporizer unit permits analysis using the reduction vaporization –– atomic absorption method. It permits easy, high-sensitivity water quality analysis. Vaporization method: reduction vaporization with a reducing agent Measurement method: recirculation Flow cell: optical path length 100 mm (with quartz window) Sample volume: 250 mL max.

• Features of the WizAArd Software The WizAArd software used with the AA-7000 runs under Windows 7/ Vista/XP. Wizard Functions Make Setting the Conditions So Simple That Even a Novice Can Do It. Measurement Screen Layout Shows Measurement Status at a Glance Just set the measurement conditions using WizAArd to complete the general settings. The initial settings can also be completed simply by following the Wizard procedures. Lamp History Function Assists with Lamp Management The accumulated

• Software Provides Comprehensive Information Displays and Flexible Settings Identical software operation for flame and furnace measurements Combining a high-performance autosampler simplifies advanced settings Even if the calibration curve is created after sample measurements, concentration calculations can be conducted on past data. This allows trial measurements to be directly used as actual measurements. Extrapolation of calibration curve range. If the sample concent

• Standard Parts / PC / Software 20 * The PC, monitor, printer, hollow cathode lamps, high-temperature burner head, pressure regulator and compressor are not included in the standard configuration. Part Name Quantity P/N 071-60821-08 (120 V), 071-60825-51 (230 V)1 206-52046-911 1 206-97176 Common to All AA-7000 Series Models 1 206-97225 1 228-30164 1 037-70238-01 1 221-40500 3 206-57770 206-777041 206-77551-121 206-84934-671 AA-7000G Stan

• AA-7000 Series Printed in Japan 3655-09416-30ANS Company names, product/service names and logos used in this publication are trademarks and trade names of Shimadzu Corporation or its affiliates, whether or not they are used with trademark symbol “TM” or “®”. Third-party trademarks and trade names may be used in this publication to refer to either the entities or their products/services. Shimadzu disclaims any proprietary i

• Pb 0.08ppb Mn 0.02ppb 0.05ppb 0.01ppb Enhanced Sensitivity due to Graphite Furnace Advances in optics and a new graphite furnace design achieve improved lower limits of detection for furnace analysis (comparison with previous Shimadzu models). This superb analysis performance is possible in all fields. Achieves World-Class Lower Limits of Detection Previous New 8 World-Class High-Sensitivity Furnace
  

• World first! –– flame extinguished automatically by vibration sensor The flame is automatically extinguished when the new built-in sensor detects vibrations. Instruments are completely safe during severe shaking caused by earthquakes. Multimode automatic gas leak check The fuel gas pipes inside the instrument gas controller are automatically checked for gas leaks when the power is turned on and when the flame is extinguished. Should a gas leak be detected, a warning buzzer sounds and a warning is displayed on the screen. Flame-ret

• Detector Hollow cathode lamp Beam splitter Monochromator D2 lamp Chopper mirror Burner head (or graphite tube) Reference beam Sample beam 6 Enhanced Flame Analysis The AA-7000 Series incorporates newly developed 3D double-beam optics. The optical system has been designed to produce its maximum performance for each measurement method through optimal adjustment of the light beam and light beam digital filter, and by using optical components that restrict light losses. Double-Beam Optics and Stable Hardware Achieve Superior Stability
  

• 7 Advantages of the Double-Beam System Support for Developing Analytical Conditions Optional Autosampler Reduces Analysis Workload Long-term stability The graph shows the results of measurements on 2 ppm copper (Cu) conducted over at least one hour. (The plot shows mean values for 11 repeated measurements.) Over the course of more than 600 measurements, the instrument achieved a relative standard deviation within 1%. High sensitivity The